The Study of the reaction of N,N-diethylhydrazine with nitrobenzoic acids
DOI:
https://doi.org/10.56042/ijc.v65i7.18956Keywords:
N,N-diethylhydrazine, nitrobenzoic acid isomers, quaternary ammonium salts, X-ray structural analysis, ion-molecular complexAbstract
In this study, the synthesis of the N,N-diethylhydrazine salt of nitrobenzoic acid isomers containing an electron-withdrawing group in the molecule was carried out, and it was found that the type of solvents, molar ratios of the starting materials, and reaction time parameters in the preparation of this N,N-diethylhydrazine salt affected the product yield. According to the results, when parameters such as molar ratios of the starting materials, solvents, temperature, and reaction time were studied, the reaction yield increased to 90%. The structure of this synthesized compound was determined using IR spectrum, 1H YAMR, and X-ray analysis.